Synthesis, Molecular Structure and Spectroscopic Studies of 6,6'-(1E,1'E)-(Ethane-1,2-Diylbis(azan-1-yl-1-ylidene))bis(Phenylmethan-1-yl-1-ylidene)bis(3-(Octyloxy)phenol)

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dc.contributor.authorTanak, Hasan
dc.contributor.authorMeral, Seher
dc.contributor.authorAgar, Aysen Alaman
dc.date.accessioned2025-03-23T19:31:38Z
dc.date.available2025-03-23T19:31:38Z
dc.date.issued2020
dc.departmentSinop Üniversitesi
dc.description.abstract6,6'-(1E,1'E)-(ethane-1,2-diylbis(azan-1-yl-1-ylidene))bis(phenylmethan-1-yl-1-ylidene)bis(3-(octyloxy)phenol) has been synthesized and characterized by FTIR, H-1, C-13 NMR and single-crystal X-ray determination. The compound crystallizes in monoclinic space group C2/c with Z = 4 in the unit cell. The asymmetric unit of the compound contains one half-organic molecule. The molecule is located about a two-fold rotation axis which bisects the central C14-C14(i) bond. The dihedral angle between the phenyl rings is 68.46(11)degrees. In the crystal, intramolecular O-H...N hydrogen bonds generates a six-membered ring, producing an S(6) ring motif. The crystal packing is also stabilized by C-H...pi interactions.
dc.description.sponsorshipResearch Centre of Ondokuz Mayis University [PYO.FEN.1904.18.003]
dc.description.sponsorshipThis study was supported financially by the Research Centre of Ondokuz Mayis University (project no. PYO.FEN.1904.18.003).
dc.identifier.doi10.1134/S1063774520070251
dc.identifier.endpage1220
dc.identifier.issn1063-7745
dc.identifier.issn1562-689X
dc.identifier.issue7
dc.identifier.scopus2-s2.0-85096522542
dc.identifier.scopusqualityQ4
dc.identifier.startpage1217
dc.identifier.urihttps://doi.org/10.1134/S1063774520070251
dc.identifier.urihttps://hdl.handle.net/11486/5326
dc.identifier.volume65
dc.identifier.wosWOS:000592546300024
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherPleiades Publishing Inc
dc.relation.ispartofCrystallography Reports
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250323
dc.subjectExperimental Xrd
dc.subjectFt-Ir
dc.subjectSchiff
dc.subjectCluster
dc.titleSynthesis, Molecular Structure and Spectroscopic Studies of 6,6'-(1E,1'E)-(Ethane-1,2-Diylbis(azan-1-yl-1-ylidene))bis(Phenylmethan-1-yl-1-ylidene)bis(3-(Octyloxy)phenol)
dc.typeArticle

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