A novel electro analytical nanosensor based on graphene oxide/silver nanoparticles for simultaneous determination of quercetin and morin

dc.authoridAtar, Necip/0000-0001-8779-1412
dc.contributor.authorYola, Mehmet Lutfi
dc.contributor.authorGupta, Vinod Kumar
dc.contributor.authorEren, Tanju
dc.contributor.authorSen, Arif Emre
dc.contributor.authorAtar, Necip
dc.date.accessioned2025-03-23T19:41:44Z
dc.date.available2025-03-23T19:41:44Z
dc.date.issued2014
dc.departmentSinop Üniversitesi
dc.description.abstractIn this report, silver nanoparticles (AgNPs) with the mean diameters of 10-30 nm were self-assembled onto the surfaces of 2-aminoethanethiol (2-AET) functionalized graphene oxide (AETGO) sheets. The graphene oxide (GO) and AgNPs-AETGO nanocomposites were characterized by a transmission electron microscope (TEM), x-ray photoelectron spectroscopy (XPS), reflection absorption infrared spectroscopy (RAIRS) and the x-ray diffraction (XRD). The simultaneous determination of quercetin (QR) and morin (MR) has been performed on glassy carbon electrode (GCE) modified with AgNPs-AETGO (AgNPs-AETGO/GCE). QR presented an oxidation step at Ea of 200 mV and reduction step at Ec of 150 mV and RT presented an oxidation step at Ea of 600 mV at AgNPs-AETGO/GCE by cyclic voltammetry (CV). The linearity ranges and the detection limits of QR and MR were 1.0 x 10-8 - 5.0 x 10-6 M and 3.3 x 10-9 M, respectively. The AgNPs-AETGO/GCE was also applied to real samples for the simultaneous determination of QR and MR. Thus the developed method can be adopted as an alternative to the published chromatographic, spectrophotometric and electroanalytical methods for simultaneous determination of QR and MR. (C) 2013 Elsevier Ltd. All rights reserved.
dc.identifier.doi10.1016/j.electacta.2013.12.086
dc.identifier.endpage211
dc.identifier.issn0013-4686
dc.identifier.issn1873-3859
dc.identifier.scopus2-s2.0-84892509496
dc.identifier.scopusqualityQ1
dc.identifier.startpage204
dc.identifier.urihttps://doi.org/10.1016/j.electacta.2013.12.086
dc.identifier.urihttps://hdl.handle.net/11486/6630
dc.identifier.volume120
dc.identifier.wosWOS:000333778200027
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherPergamon-Elsevier Science Ltd
dc.relation.ispartofElectrochimica Acta
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250323
dc.subjectQuercetin
dc.subjectMorin
dc.subjectGraphene oxide
dc.subjectSilver nanoparticles
dc.subjectSquare wave voltammetry
dc.titleA novel electro analytical nanosensor based on graphene oxide/silver nanoparticles for simultaneous determination of quercetin and morin
dc.typeArticle

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