Synthesis, spectroscopic, and molecular structure characterizations of some azo derivatives of 2-hydroxyacetophenone

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dc.authoridAlbayrak kastas, Cigdem/0000-0003-0235-7460
dc.contributor.authorAlbayrak, Cigdem
dc.contributor.authorGumrukcuoglu, Ismail E.
dc.contributor.authorOdabasoglu, Mustafa
dc.contributor.authorIskeleli, Nazan Ocak
dc.contributor.authorAgar, Erbil
dc.date.accessioned2025-03-23T19:40:51Z
dc.date.available2025-03-23T19:40:51Z
dc.date.issued2009
dc.departmentSinop Üniversitesi
dc.description.abstractSome novel azo compounds were prepared by the reaction of 2-hydroxyacetophenone with aniline and its substituted derivatives. The structures of synthesized azo compounds were determined by IR, UV-Vis, H-1 NMR and C-13 NMR spectroscopic techniques and the structures of some of these compounds were also determined by X-ray diffraction studies. Structural analysis using IR in solid state shows that the azo form is favoured in the azo compounds whereas UV-Vis analysis of the azo compounds in solution has shown that there is a azo and ionic form. The azo compounds in the basic solvents dimethylformamide (DMF) and dimethylsulfoxide (DMSO) are both azo and ionic form while these compounds in ethyl alcohol (EtOH) and chloroform (CHCl3) are only azo form. (C) 2009 Elsevier B.V. All rights reserved.
dc.identifier.doi10.1016/j.molstruc.2009.05.043
dc.identifier.endpage54
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.issue1-3
dc.identifier.scopus2-s2.0-67650474758
dc.identifier.scopusqualityQ1
dc.identifier.startpage43
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2009.05.043
dc.identifier.urihttps://hdl.handle.net/11486/6432
dc.identifier.volume932
dc.identifier.wosWOS:000268652900006
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofJournal of Molecular Structure
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250323
dc.subjectAzobenzene
dc.subjectAzo dyes
dc.subjectX-ray analysis
dc.subjectSpectral characterization
dc.subject2-Hydroxyacetophenone
dc.titleSynthesis, spectroscopic, and molecular structure characterizations of some azo derivatives of 2-hydroxyacetophenone
dc.typeArticle

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