Electrochemically modified sulfisoxazole nanofilm on glassy carbon for determination of cadmium(II) in water samples

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dc.authoridUzun, Lokman/0000-0002-3971-7725
dc.authoridUstundag, Zafer/0000-0002-5550-106X
dc.authoridAtar, Necip/0000-0001-8779-1412
dc.contributor.authorGupta, Vinod Kumar
dc.contributor.authorYola, Mehmet Lutfi
dc.contributor.authorAtar, Necip
dc.contributor.authorSolak, Ali Osman
dc.contributor.authorUzun, Lokman
dc.contributor.authorUstundag, Zafer
dc.date.accessioned2025-03-23T19:41:45Z
dc.date.available2025-03-23T19:41:45Z
dc.date.issued2013
dc.departmentSinop Üniversitesi
dc.description.abstractSulfisoxazole (SO) was grafted to glassy carbon electrode (GCE) via the electrochemical oxidation of SO in acetonitrile solution containing 0.1 M tetrabutylammoniumtetra-fluoroborate (TBATFB). The prepared electrode was characterized by using cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), reflection-absorption infrared spectroscopy (RAIRS) and X-ray photoelectron spectroscopy (XPS). The ellipsometric thickness of SO nanofilm at the glassy carbon surface was obtained as 14.48 +/- 0.11 nm. The stability of the SO modified GCE was studied. The SO modified GCE was also utilized for the determination of Cd(II) ions in water samples in the presence of Pb(II) and Fe(II) by adsorptive stripping voltammetry. The linearity range and the detection limit of Cd(II) ions were 1.0 x 10(-1) to 5.0 x 10(-8) M and 3.3 x 10(-11) M (S/N = 3), respectively. (C) 2013 Elsevier Ltd. All rights reserved.
dc.identifier.doi10.1016/j.electacta.2013.04.136
dc.identifier.endpage156
dc.identifier.issn0013-4686
dc.identifier.issn1873-3859
dc.identifier.scopus2-s2.0-84878309858
dc.identifier.scopusqualityQ1
dc.identifier.startpage149
dc.identifier.urihttps://doi.org/10.1016/j.electacta.2013.04.136
dc.identifier.urihttps://hdl.handle.net/11486/6634
dc.identifier.volume105
dc.identifier.wosWOS:000322414800021
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherPergamon-Elsevier Science Ltd
dc.relation.ispartofElectrochimica Acta
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250323
dc.subjectSulfisoxazole
dc.subjectModification
dc.subjectSurface characterization
dc.subjectNanofilm
dc.subjectCd(II) ion detection
dc.titleElectrochemically modified sulfisoxazole nanofilm on glassy carbon for determination of cadmium(II) in water samples
dc.typeArticle

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