Arsenic speciation in water and biota samples at trace levels by ion chromatography inductively coupled plasma-mass spectrometry

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dc.authoridCHORMEY, DOTSE SELALI/0000-0002-7412-7800
dc.authoridElkiran, Omer/0000-0003-1933-4003
dc.contributor.authorFirat, Merve
dc.contributor.authorBakirdere, Sezgin
dc.contributor.authorSel, Sabriye
dc.contributor.authorChormey, Dotse Selali
dc.contributor.authorElkiran, Omer
dc.contributor.authorErulas, Fatih
dc.contributor.authorTurak, Fatma
dc.date.accessioned2025-03-23T19:35:17Z
dc.date.available2025-03-23T19:35:17Z
dc.date.issued2017
dc.departmentSinop Üniversitesi
dc.description.abstractA sensitive, reliable, simple and rapid analytical method was developed for the determination of arsenite [As(III)], arsenate [As(V)] and arsenobetaine (AsB) species using ion chromatography combined with inductively coupled plasma-mass spectrometry (IC-ICP-MS). Inorganic and organic arsenic species were separated with an anion exchange column (Dionex AS9) and a 50mM sodium bicarbonate mobile phase (pH 10) at a flow rate of 1.0mL min(-1.) %RSD values were found to be lower than 5.1% for all arsenic species. The limits of detection (LOD) obtained for As(III), As(V) and AsB were 16.5 ng L-1, 14.1 ng L-1 and 6.2 ng L-1, respectively. The developed analytical method was tested using AsB certified reference material (NMIJ CRM 7901-a), and spring water certified reference material (UME CRM 1201) for accuracy check. This method was applied for the quantitative determination of arsenic species in different water samples and chicken samples as a solid matrix.
dc.identifier.doi10.1080/03067319.2017.1346089
dc.identifier.endpage693
dc.identifier.issn0306-7319
dc.identifier.issn1029-0397
dc.identifier.issue7
dc.identifier.scopus2-s2.0-85022086211
dc.identifier.scopusqualityQ1
dc.identifier.startpage684
dc.identifier.urihttps://doi.org/10.1080/03067319.2017.1346089
dc.identifier.urihttps://hdl.handle.net/11486/5831
dc.identifier.volume97
dc.identifier.wosWOS:000405810200007
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis Ltd
dc.relation.ispartofInternational Journal of Environmental Analytical Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250323
dc.subjectArsenic
dc.subjectspeciation
dc.subjectIC-ICP-MS
dc.subjectwater
dc.subjectchicken
dc.titleArsenic speciation in water and biota samples at trace levels by ion chromatography inductively coupled plasma-mass spectrometry
dc.typeArticle

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