Spectroscopic Properties and Preparation of Some 2,3-Dimethoxybenzamide Derivatives

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dc.authoridCAKMAK, Sukriye/0000-0002-2221-0098
dc.authoridYAKAN, HASAN/0000-0002-4428-4696
dc.contributor.authorCakmak, Sukriye
dc.contributor.authorKutuk, Halil
dc.contributor.authorOdabasoglu, Mustafa
dc.contributor.authorYakan, Hasan
dc.contributor.authorBuyukgungor, Orhan
dc.date.accessioned2025-03-23T19:27:14Z
dc.date.available2025-03-23T19:27:14Z
dc.date.issued2016
dc.departmentSinop Üniversitesi
dc.description.abstractIn this study, a series of substituted secondary amide compounds were synthesized starting from 2,3-dimethoxybenzoic acid and aniline derivatives. The structures of these synthesized compounds were determined using IR, H-1 NMR and C-13 NMR spectroscopy, X-ray diffraction and elemental analysis techniques. Background: Amides are important groups in organic compounds. Amides moieties are found in many natural products. We now report a complementary study of the amide derivatives and the structures of these synthesized compounds were determined using IR, H-1 NMR and C-13 NMR spectroscopy, X- ray diffraction and elemental analysis techniques. Methods: Substituted secondary amides were prepared from the corresponding 2,3-dimethoxybenzoic acid. This involved reaction of 2,3-dimethoxybenzoyl chloride with the appropriate aniline derivatives in the presence of THF to give substituted secondary amides. Results: A summary of crystallographic data, experimental details, and refinement results for compounds are given. Conclusion: In this study a simple, yet effective method was used for the synthesis of some benzamides from acyl chlorides with aniline and its derivatives in the presence of triethylamine. All the products were obtained with moderate-good yields.
dc.description.sponsorshipOndokuz Mayis University [PYO.FEN.1904.12.007]
dc.description.sponsorshipWe would like to thank Ondokuz Mayis University (Grant No. PYO.FEN.1904.12.007) for its financial support of this work.
dc.identifier.doi10.2174/1570178613666151230210931
dc.identifier.endpage194
dc.identifier.issn1570-1786
dc.identifier.issn1875-6255
dc.identifier.issue3
dc.identifier.scopus2-s2.0-84958760336
dc.identifier.scopusqualityQ4
dc.identifier.startpage181
dc.identifier.urihttps://doi.org/10.2174/1570178613666151230210931
dc.identifier.urihttps://hdl.handle.net/11486/4870
dc.identifier.volume13
dc.identifier.wosWOS:000373936500004
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherBentham Science Publ Ltd
dc.relation.ispartofLetters in Organic Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WOS_20250323
dc.subjectAcyl chloride
dc.subjectaniline derivatives
dc.subjectbenzamides
dc.subjectsecondary amides
dc.subjectspectroscopic properties
dc.subjectX-ray diffraction
dc.titleSpectroscopic Properties and Preparation of Some 2,3-Dimethoxybenzamide Derivatives
dc.typeArticle

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