Synthesis and Characterization of a New Nickel(II) Compound Derived from [BW12O40]3- and 2,2'-Bipyridyl
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Tarih
2020
Dergi Başlığı
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Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
A Keggin-type polyoxometalate {Ni(2,2'-bipy)2(H2O)[BW12O40]}3- (NiBWO) has been hydrothermallysynthesized in the high temperature resistant glass bottle for the first time. The structure has beencharacterized.by elemental analyses, X-ray diffraction, Fourier Transform Infrared Spectroscopy,Thermogravimetric Analysis, Scanning Electron Microscope and X-ray single crystal diffraction analyses.The X-ray single crystal study shows that the asymmetric unit of NiBWO is composed of one [BW12O40]5-anion, one [Ni(2,2'-bipy)2(H2O)]2+ and one and a half of [Ni(2,2'-bipy)3]2+ cations.
Açıklama
Anahtar Kelimeler
Kimya, İnorganik ve Nükleer
Kaynak
Afyon Kocatepe Üniversitesi Fen ve Mühendislik Bilimleri Dergisi
WoS Q Değeri
Scopus Q Değeri
Cilt
20
Sayı
4
