Synthesis of some symmetric disulfides from thiophthalimides and amines under microwave irradiation

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dc.contributor.authorYakan, Hasan
dc.contributor.authorKarakullukcu, Nalan Turkoz
dc.contributor.authorCakmak, Sukriye
dc.contributor.authorKutuk, Halil
dc.date.accessioned2025-03-23T19:17:48Z
dc.date.available2025-03-23T19:17:48Z
dc.date.issued2018
dc.departmentSinop Üniversitesi
dc.description.abstractSome symmetric disulfides have been astonishingly prepared from thiophthalimides (sulfenimides) and amines in the presence of 2-ethoxyethanol (β-ee, neat) at microwave irradiation under free catalyst and ligand. The products were obtained in good to excellent yields ranging from 62% to 92%. When only thiophthalimides were exposed to microwave irradiation, disulfides were not obtained. Also, disulfides were not obtained from thiophthalimides in the presence of 2-ethoxyethanol (neat) under microwave irradiation. We compared the microwave-assisted synthesis method with the classical method. The products obtained were purified with chromatographic method and the analysis of them was performed with IR, 1H NMR, 13C NMR spectroscopic and elemental methods. © 2018 World Research Association. All rights reserved.
dc.description.sponsorshipOndokuz Mayis Üniversitesi, (PYO.FEN.1904.10.024)
dc.identifier.endpage54
dc.identifier.issn0972-0626
dc.identifier.issue4
dc.identifier.scopus2-s2.0-85044532198
dc.identifier.scopusqualityQ4
dc.identifier.startpage45
dc.identifier.urihttps://hdl.handle.net/11486/4433
dc.identifier.volume22
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherWorld Research Association
dc.relation.ispartofResearch Journal of Chemistry and Environment
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_Scopus_20250323
dc.subject2-Ethoxyethanol
dc.subjectDisulfides
dc.subjectMicrowave heating
dc.subjectSulfenimides
dc.titleSynthesis of some symmetric disulfides from thiophthalimides and amines under microwave irradiation
dc.typeArticle

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