Synthesis and Properties of Triazol-5-one Substituted Phthalocyanines by Microwave Irradiation

dc.contributor.authorKahveci, Bahittin
dc.contributor.authorŞaşmaz, Selami
dc.contributor.authorÖzil, Musa
dc.contributor.authorKantar, Cihan
dc.contributor.authorKoşar, Başak
dc.contributor.authorBüyükgüngör, Orhan
dc.date.accessioned2014-08-11T12:36:51Z
dc.date.available2014-08-11T12:36:51Z
dc.date.issued2006
dc.description.abstractTriazol-5-one substituted phthalocyanines were prepared quickly by the reaction of 4-nitrophthalonitrile with anhydrous metal salts in DBU (1,8-diazabicyclo[5,4,0]undec-7-ene) and DMAE (dimethylaminoethanol) by microwave irradiation. Microwave yields were higher than those of the conventional synthesis methods. All of these complexes are insoluble in polar solvents such as ethanol, ethyl acetate and chloroform. The characterization of the compounds was accomplished by elemental analysis, 1H NMR (for I and II), 13C NMR (for I and II), IR and UV-Vis spectral data. In addition, the structure of the starting material (I) was determined by single crystal diffraction.
dc.identifier.citationKahveci, B., Şaşmaz, S., Özil, M., Kantar, C., Koşar, B., Büyükgüngör, O. "Synthesis and Properties of Triazol-5-one Substituted Phthalocyanines by Microwave Irradiation" Turkish Journal of Chemistry, 30 (2006) , 681 – 689.
dc.identifier.urihttp://journals.tubitak.gov.tr/chem/issues/kim-06-30-6/kim-30-6-4-0512-27.pdf
dc.identifier.urihttps://hdl.handle.net/11486/278
dc.language.isoen
dc.publisherTurkish Journal of Chemistry
dc.relation.publicationcategoryMakale - Kategorisiz
dc.subjectPhthalocyanine
dc.subjectMicrowave synthesis
dc.titleSynthesis and Properties of Triazol-5-one Substituted Phthalocyanines by Microwave Irradiation
dc.typeArticle

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