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Öğe Hydro/ Solvothermal Synthesis and Crystal Structure of New Ni(II) Coordination Polymer Containing Pamoic Acid and Ethylenediamine Mixed Ligands : {[Ni(µ-pam)(en)2]·H2O}n(2017) Tümer, Yasemin; Şahin, OnurThe new coordination polymers arranged from flexible pamoic acid, namely {[Ni(µ-pam)(en)2]·H2O}n (1), (H2pam= pamoic acid, en= ethylenediamine), have been synthesized under hydro/ solvothermal conditions and characterized by elemental analysis, simultaneous TG, DTA techniques, IR spectroscopy, and X-ray crystallography. X-ray single crystal structure analysis of 1 shows that the Ni(II) ions are bridged by pamoic acid ligands to generate 1-dimensional (1D) coordination polymer running parallel to the direction, with the Ni∙∙∙Ni separation is 14.057 Å. Adjacent 1D chains are connected by N-H···O and O-H···O hydrogen bonds to establishing 3 dimensional (3D) supramolecular networkÖğe The synthesis of new phosphazene-bearing ethyl p-hydroxybenzoate and ferrocenyl pendant groups and their spectroscopic and crystallographic characterizations(Turkish Chemical Society, 2020) Tümer, Yasemin; Çayırbaşı, Mahmut; Şahin, Onur; Hökelek, TuncerThis is a study of new hexachlorocyclotriphosphazene (N3P3Cl6) derivatives bearing ethyl p-hydroxybenzoate and ferrocenyl pendant groups. Characterizations of the products [mono-2, di-(geminal 3a; non-geminal transa-3b, transb-3c and cis-3d), tri-4 and tetra-5 substituted phosphazene derivatives] were performed using elemental analysis and spectral methods. The structures of the two compounds (2 and 5) were explained by the use of X-ray diffraction techniques. © 2020, Turkish Chemical Society. All rights reserved.Öğe The Synthesis of New Phosphazene-Bearing Ethyl pHydroxybenzoate and Ferrocenyl Pendant Groups and their Spectroscopic and Crystallographic Characterizations(2020) Tümer, Yasemin; Çayırbaşı, Mahmut; Şahin, Onur; Hokelek, TuncerThis is a study of new hexachlorocyclotriphosphazene (N3P3Cl6) derivatives bearing ethylp-hydroxybenzoate and ferrocenyl pendant groups. Characterizations of the products [mono- 2, di-(geminal 3a; non-geminal transa-3b, transb-3c and cis-3d), tri- 4 and tetra- 5 substitutedphosphazene derivatives] were performed using elemental analysis and spectral methods. Thestructures of the two compounds (2 and 5) were explained by the use of X-ray diffractiontechniques.
