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    Crystal structure of N-2-methoxyphenyl-2-oxo-5-nitro-1-benzylidenemethylamine
    (Japan Society for Analytical Chemistry, 2008) Tanak, Hasan; Erşahin, Ferda; Aar, Erbil; Büyükgüngör, Orhan; Yavuz, Metin
    The crystal structure of the title compound, C14H12N2O4, was determined by a single-crystal X-ray diffraction technique, (Fig. 1). The title compound crystallizes in the orthorhombic space group Pca21 with the following unit-cell parameters: a = 18.4391(15)Å, b = 4.2710(2)Å, c = 32.2187(16)Å and V = 2537.3(3)Å3. The crystal data were solved with a final R = 0.062 using 2394 independent reflections. There are two molecules in the asymmetric unit. The title compound adopts the keto-amine tautomeric form. In the structure, there are N-H...O and C-H ···O intramolecular hydrogen bonds and C-H · · ·O intermolecular hydrogen bonds. 2008 © The Japan Society for Analytical Chemistry.