Uçar, AsumanFındık, MükerremKocak, NuriyeÇolak, Alper TolgaŞahin, Onur2025-03-232025-03-2320212587-26802587-246Xhttps://doi.org/10.17776/csj.812164https://search.trdizin.gov.tr/tr/yayin/detay/1120627https://hdl.handle.net/11486/3693Herein a novel inorganic-organic hybrid Keggin-type heteropolymolybdate [Ni2Na(C12H8N2)4(BMo12O40)(H2O)2] (1) has been synthesized under hydrothermal conditions in aqueous solution. The cyrstal structure was fully characterized by powder X-ray diffraction (XRD), elemental analysis, Fourier-tranform infrared spectrum (FT-IR), Thermogravimetric analysis (TGA) and Scanning Electron Microscopy (SEM) analysis. Single crystal X-ray structural analysis demonstrates that the complex consists of a Keggin anion [BMo12O40]5− polyanion, four 1,10-phenanthroline (C12H8N2) ligands, two Ni(II) ions, two Na(I) ions and two aqua ligands. The experimental powder X-ray diffraction (XRD) result of the crystal is consistent with the calculated data. The SEM image shows that the compound crystals have a cubic structure.eninfo:eu-repo/semantics/openAccessKimyaİnorganik ve NükleerArticle421222910.17776/csj.8121641120627