Fındık, MükerremUçar, AsumanKocak, NuriyeŞahin, OnurÇolak, Alper Tolga2025-03-232025-03-2320202149-3367https://doi.org/10.35414/akufemubid.762026https://search.trdizin.gov.tr/tr/yayin/detay/367506https://hdl.handle.net/11486/3270A Keggin-type polyoxometalate {Ni(2,2'-bipy)2(H2O)[BW12O40]}3- (NiBWO) has been hydrothermallysynthesized in the high temperature resistant glass bottle for the first time. The structure has beencharacterized.by elemental analyses, X-ray diffraction, Fourier Transform Infrared Spectroscopy,Thermogravimetric Analysis, Scanning Electron Microscope and X-ray single crystal diffraction analyses.The X-ray single crystal study shows that the asymmetric unit of NiBWO is composed of one [BW12O40]5-anion, one [Ni(2,2'-bipy)2(H2O)]2+ and one and a half of [Ni(2,2'-bipy)3]2+ cations.eninfo:eu-repo/semantics/openAccessKimyaİnorganik ve NükleerArticle20457658110.35414/akufemubid.762026367506